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| Registros recuperados : 11 | |
| 2. |  | PALLADINO, C.; PAREJA, L.; PEREYRA, S.; PÉREZ, C. Problems of pesticide residues in grains. [La problemática de los residuos de fitosanitarios en granos]. [Problemática dos resíduos de fitossanitários em grãos]. I Technical Conference of the Plant Protection Group - EEMAC. Agrociencia Uruguay, 2023, Vol.27 (Supplement), e1230. https://doi.org/10.31285/AGRO.27.1230 -- OPEN ACCESS. Article history: Received 24 Jul 2032; Accepted 25 Jul 2023; Published 11 Sep 2023. -- Editor: Horacio Silva, Universidad de la República, Facultad de Agronomía, Paysandú, Uruguay. -- Correspondence: Cintia Palladino,...| Biblioteca(s): INIA Las Brujas. |
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| 3. | | PALLADINO, C.; PÉREZ, C.A.; PAREJA, L.; PÉREZ-PARADA. A.; FRANCO, J.; PEREYRA, S. Fungicide strategies for Ramularia Leaf Spot control recommended in Uruguay and its residues in barley grains. [Estrategias de fungicidas recomendadas para el control de ramulariosis en Uruguay y sus residuos en granos de cebada.]. [Estratégias de fungicidas para o controlo da ramulariose recomendadas no Uruguai e respectivos resíduos nos grãos de cevada.]. Section. Plant protection. Agrociencia Uruguay, 2024, Vol.28, e1262. https://doi.org/10.31285/AGRO.28.1262 -- OPEN ACCESS. Article history: Received 04 October 2023; Accepted 01 December 2023; Published 01 February 2024. -- Editor: María Inés Siri, Universidad de la República, Montevideo, Uruguay. -- Correspondence: Cintia Palladino, cpalladino@cup.edu.uy --...| Biblioteca(s): INIA Las Brujas. |
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| 5. | | PALLADINO, C.; MUELA, A.; TABORDA, B.; PUIGVERT, F.; PÉREZ-PARADA, A.; COLAZZO, M.; PÉREZ, C. A.; PEREYRA, S.; PAREJA, L. Application of a straightforward Mmthodology by LC-QqQ-MS/MS and GC-MS to ensure food safety of barley and wheat grain. ACS Agricultural Science and Technology, 2022, Volume 2, Issue 2, Pages 371-380. doi: https://doi.org/10.1021/acsagscitech.1c00263 Article history: Received 29 November 2021; Accepted 24 February 2022; Revised 4 February 2022; Published online 16 March 2022; Published in issue 18 April 2022.
Corresponding author: Pareja, L.; Departamento de Química Del...| Biblioteca(s): INIA Las Brujas. |
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| 6. | | PAREJA, L.; COLAZZO, M.; PÉREZ-PARADA, A.; NIELL, S.; CARRASCO-LETELIER, L.; BESIL, N.; CESIO, M.V.; HEINZEN, H. Detection of pesticides in active and depopulated beehives in Uruguay International Journal of Environmental Research and Public Health, 2011, v. 8, n. 10, p. 3844-3858 OPEN ACCESS ARTICLE.| Biblioteca(s): INIA La Estanzuela; INIA Las Brujas. |
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| 7. | | NIELL, S.; PAREJA, L.; ASTEGGIANTE, L.G.; ROEHRS, R.; PIZZUTTI, I.R.; GARCIA, C.; HEINZEN, H.; CESIO, M.V. Development of methods for multiresidue analysis of rice post-emergence herbicides in loam soil and their possible applications to soils of different composition. Journal of AOAC International, 2010, v. 93 no.2, p. 425-431. 2-s2.0-77952781014| Biblioteca(s): INIA Las Brujas. |
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| 8. | | Cesio, V.; Pareja, L.; Niell, S.; Geis Asteggiante, L.; Bocking, B.; García, C.; Fernández, G.; Fernández-Alba, A.R.; Heinzen, H. Critical revision and development perspectives of herbicide residues analysis in Agro Ecosystems 1a.ed. ln: Kortekamp, A. (ed). Herbicides and environment. India: Intech, 2011. p.125-156| Biblioteca(s): INIA Las Brujas. |
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| 9. | | NIELL, S.; JESÚS, F.; PÉREZ, N.; PÉREZ, C.; PAREJA, L.; ABATTE, S.; CARRASCO-LETELIER, L.; DIAZ, S.; MENDOZA, Y.; CESIO, V.; HEINZEN, H. Neonicotinoids transference from the field to the hive by honey bees: Towards a pesticide residues biomonitor Science of the Total Environment, 2017, v. 581-582, p. 25-31 Article history: Received 3 October 2016 / Received in revised form 14 December 2016 / Accepted 2 January 2017 / Available online xxxx| Biblioteca(s): INIA La Estanzuela; INIA Las Brujas. |
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| 10. | | PÉREZ, A.; ALONSO, B.; ERNST, F.; RODRÍGUEZ, C.; CESIO, V.; HEINZEN, H.; COLAZZO, M.; PAREJA, L.; PEREIRA, A.; MÁRQUEZ, A.; ERRICO, E. Residuos de plaguicidas en compartimentos ambientales. Montevideo (UY): INIA, 2020. 30 p. (Serie FPTA-INIA; 90) Proyecto FPTA 324: "Estudio del impacto de las actuales prácticas agrícolas en los recursos hídricos del bajo Río Negro y Esteros de Farrapos.". Período de ejecución: Mayo 2014 - Junio 2017. Institución Ejecutora: Universidad de la...| Biblioteca(s): INIA Las Brujas. |
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| 11. | | PEREYRA, S.; CASTRO, M.; VERO, S.; SILVA, P.; CAL, A.; TISCORNIA, G.; GONZALEZ, N.; BENTOS, D.; ALVAREZ, W.; RABAZA, S.; SEVILLANO, L.; BRANCATTI, G.; FRANCIA, C.; RAFFO, M.A.; GERMAN, S.; PÉREZ, C.; GARMENDIA, G.; PAREJA, L.; RODRÍGUEZ, A.; PENDAS, C.; QUINCKE, M.; VÁZQUEZ, D.; RODRIGUEZ, M. Fusariosis de la espiga en trigo y micotoxinas asociadas: contribuyendo a reducir su riesgo. Cultivos. Revista INIA Uruguay, Diciembre 2023, no.75 p.54-58. (Revista INIA; 75).| Biblioteca(s): INIA Las Brujas. |
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| Registros recuperados : 11 | |
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 | Acceso al texto completo restringido a Biblioteca INIA Las Brujas. Por información adicional contacte bibliolb@inia.org.uy. |
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Registro completo
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Biblioteca (s) : |
INIA Las Brujas. |
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Fecha actual : |
25/10/2014 |
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Actualizado : |
03/10/2019 |
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Tipo de producción científica : |
Artículos en Revistas Indexadas Internacionales |
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Circulación / Nivel : |
B - 1 |
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Autor : |
NIELL, S.; PAREJA, L.; ASTEGGIANTE, L.G.; ROEHRS, R.; PIZZUTTI, I.R.; GARCIA, C.; HEINZEN, H.; CESIO, M.V. |
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Afiliación : |
SILVINA NIELL, Universidad de la República, Farmacognosia y Productos Naturales. Uruguay; LUCÍA PAREJA, Universidad de la República, Farmacognosia y Productos Naturales. Uruguay; LUCA GEIS ASTEGGIANTE, Universidad de la República, Farmacognosia y Productos Naturales. Uruguay; RAFAEL ROEHRS, LARP/Universidade Federal de Santa Maria, Rio Grande do Sul, Brazil.; IONARA R. PIZZUTTI, CEPARC/Universidade Federal de Santa Maria, Rio Grande do Sul, Brazil.; CLAUDIO CESAR GARCIA GALLARRETA, Instituto Nacional de Investigación Agropecuaria (INIA), Uruguay; HORACIO HEINZEN, Universidad de la República, Farmacognosia y Productos Naturales. Uruguay; MARA VERNICA CESIO, Universidad de la República, Farmacognosia y Productos Naturales. Uruguay. |
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Título : |
Development of methods for multiresidue analysis of rice post-emergence herbicides in loam soil and their possible applications to soils of different composition. |
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Fecha de publicación : |
2010 |
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Fuente / Imprenta : |
Journal of AOAC International, 2010, v. 93 no.2, p. 425-431. |
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Descripción física : |
2-s2.0-77952781014 |
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ISSN : |
1060-3271 |
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Idioma : |
Inglés |
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Contenido : |
ABSTRACT,
Two simple and straightforward sample preparation methods were developed for the multiresidue analysis of post-emergence herbicides in loam soil that are commonly used in rice crop cultivation. A number of strategic soil extraction and cleanup methods were evaluated. The instrumental analysis was performed by HPLC with a diode array detector. The best compromise between the recoveries (69-98%) and good repeatability (RSD <15%) was obtained using either methanol or methanol-ethyl acetate (70 + 30, v/v) as extraction solvents without any further cleanup. For the first time, residues of metsulfuron methyl, bensulfuron ethyl, bentazone, cyhalofop butyl, pyrazosulfuron ethyl, propanil, and clomazone were analyzed simultaneously. Quinclorac and bispyribac sodium were also assayed, but their recoveries were below 50%. Both methods had an LOD of 0.7 ?g/kg and could accurately determine the residues at the 2 ?g/kg level. These two methods could not be applied directly to other soil types as the recoveries strongly depended on the soil composition. The developed methodologies were successfully applied in monitoring 87 real-world soil samples, in which only propanil (6 to 12 ?g/kg) and clomazone (15 to 20 ?g/kg) residues could be detected. |
|
Thesagro : |
ANÁLISIS DE SUELOS; ANÁLISIS QUÍMICO; ARROZ; SUELOS. |
|
Asunto categoría : |
P33 Química y física del suelo |
|
Marc : |
LEADER 02103naa a2200277 a 4500
001 1051310
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008 2010 bl uuuu u00u1 u #d
022 $a1060-3271
100 1 $aNIELL, S.
245 $aDevelopment of methods for multiresidue analysis of rice post-emergence herbicides in loam soil and their possible applications to soils of different composition.$h[electronic resource]
260 $c2010
300 $c2-s2.0-77952781014
520 $aABSTRACT, Two simple and straightforward sample preparation methods were developed for the multiresidue analysis of post-emergence herbicides in loam soil that are commonly used in rice crop cultivation. A number of strategic soil extraction and cleanup methods were evaluated. The instrumental analysis was performed by HPLC with a diode array detector. The best compromise between the recoveries (69-98%) and good repeatability (RSD <15%) was obtained using either methanol or methanol-ethyl acetate (70 + 30, v/v) as extraction solvents without any further cleanup. For the first time, residues of metsulfuron methyl, bensulfuron ethyl, bentazone, cyhalofop butyl, pyrazosulfuron ethyl, propanil, and clomazone were analyzed simultaneously. Quinclorac and bispyribac sodium were also assayed, but their recoveries were below 50%. Both methods had an LOD of 0.7 ?g/kg and could accurately determine the residues at the 2 ?g/kg level. These two methods could not be applied directly to other soil types as the recoveries strongly depended on the soil composition. The developed methodologies were successfully applied in monitoring 87 real-world soil samples, in which only propanil (6 to 12 ?g/kg) and clomazone (15 to 20 ?g/kg) residues could be detected.
650 $aANÁLISIS DE SUELOS
650 $aANÁLISIS QUÍMICO
650 $aARROZ
650 $aSUELOS
700 1 $aPAREJA, L.
700 1 $aASTEGGIANTE, L.G.
700 1 $aROEHRS, R.
700 1 $aPIZZUTTI, I.R.
700 1 $aGARCIA, C.
700 1 $aHEINZEN, H.
700 1 $aCESIO, M.V.
773 $tJournal of AOAC International, 2010$gv. 93 no.2, p. 425-431.
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